NMR of Quadrupolar Nuclei in Solid Materials

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Over the past 20 years technical developments in superconductingmagnet technology and instrumentation have increased the potentialof NMR spectroscopy so that it is now possible to study a widerange of solid materials. In addition, one can probe the nuclearenvironments of many other additional atoms that possess theproperty of spin. In particular, it is possible to carry out NMRexperiments on isotopes that have nuclear spin greater that ½(i.e. quadrupolar nuclei). Since more that two-thirds of allNMR active isotopes are quadrupolar nuclei, applications of NMRspectroscopy with quadrupolar nuclei are increasing rapidly.
The purpose of this handbook is to provide under a single coverthe fundamental principles, techniques and applications ofquadrupolar NMR as it pertains to solid materials. Each chapter hasbeen prepared by an expert who has made significant contributionsto out understanding and appreciation of the importance of NMRstudies of quadrupolar nuclei in solids. The text is divided intothree sections: The first provides the reader with the backgroundnecessary to appreciate the challenges in acquiring andinterpreting NMR spectra of quadrupolar neclei in solids. Thesecond presents cutting-edge techniques and methodology foremploying these techniques to investigate quadrupolar nuclei insolids. The final section explores applications of solid-state NMRstudies of solids ranging from investigations of dynamics,characterizations of biological samples, organic and inorganicmaterials, porous materials, glasses, catalysts, semiconductors andhigh-temperature superconductors.
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