Radiochemical Syntheses, Volume 2

Name: Radiochemical Syntheses, Volume 2 | Further Radiopharmaceuticals for Positron Emission Tomography and New Strategies for Their Production
Brand: Wiley
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Further Radiopharmaceuticals for Positron Emission Tomography and New Strategies for Their Production

Peter J. H. Scott(Herausgeber*in)

Wiley (Verlag)

Erschienen am 5. Mai 2015

288 Seiten

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978-1-118-83400-8 (ISBN)

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Inhalt

Intro
Title Page
Copyright Page
Contents
Radiochemical Syntheses
Contributors
Editorial Preface
Abbreviations
PART I FLUORINE-18 LABELED RADIOPHARMACEUTICALS
Chapter 1 Synthesis of (-)-[18F]Flubatine ([18F]FLBT)
1 INTRODUCTION
2 SYNTHESIS PROCEDURES
3 QUALITY CONTROL PROCEDURES
WASTE DISPOSAL INFORMATION
CHEMICAL ABSTRACTS NOMENCLATURE (REGISTRY NUMBER)
REFERENCES AND NOTES
Chapter 2 Synthesis of [18F]-(-)Fluoroethoxy Benzovesamicol ([18F]FEOBV)
1 INTRODUCTION
2 SYNTHESIS PROCEDURES
3 QC PROCEDURES
WASTE DISPOSAL INFORMATION
CHEMICAL ABSTRACTS NOMENCLATURE (REGISTRY NUMBER)
REFERENCES AND NOTES
Chapter 3 Synthesis of [18F]Fluoromethylcholine ([18F]FCH) via [18F]Fluoromethyl Tosylate
1 INTRODUCTION
2 SYNTHESIS PROCEDURES
3 QUALITY CONTROL
WASTE DISPOSAL INFORMATION
CHEMICAL ABSTRACTS NOMENCLATURE (REGISTRY NUMBER)
REFERENCES AND NOTES
Chapter 4 Radiosynthesis of [18F]Flotegatide ([18F]RGD-K5)
1 INTRODUCTION
2 SYNTHESIS PROCEDURES
3 QUALITY CONTROL PROCEDURES
WASTE DISPOSAL INFORMATION
CHEMICAL ABSTRACTS NOMENCLATURE (REGISTRY NUMBER)
REFERENCES AND NOTES
Chapter 5 Synthesis of 3-[18F]Fluoro-5-(2-Pyridinylethynyl)Benzonitrile ([18F]FPEB)
1 INTRODUCTION
2 SYNTHESIS PROCEDURES
3 QUALITY CONTROL PROCEDURES
WASTE DISPOSAL INFORMATION
CHEMICAL ABSTRACT NOMENCLATURE (REGISTRY NUMBER)
REFERENCES AND NOTES
Chapter 6 Radiosynthesis of 2'-Deoxy-2'-[18F]Fluoro-5-Methyl- 1-ß-d-Arabinofuranosyluracil ([18F]FMAU)
1 INTRODUCTION
2 SYNTHESIS PROCEDURES
3 QC PROCEDURES
WASTE DISPOSAL INFORMATION
CHEMICAL ABSTRACTS NOMENCLATURE (REGISTRY NUMBER)
REFERENCES AND NOTES
PART II CARBON-11 LABELED RADIOPHARMACEUTICALS
Chapter 7 Synthesis of N-[11C]Methyl-4-Piperidinyl Propionate ([11C]PMP)
1 INTRODUCTION
2 SYNTHESIS PROCEDURES
3 QUALITY CONTROL PROCEDURES
WASTE DISPOSAL INFORMATION
REFERENCES AND NOTES
Chapter 8 Synthesis of 1-(2,4-Dichlorophenyl)-4-Cyano-5-(4-[11C]methoxyphenyl)-N-(Piperidin-1-yl)-1H-Pyrazole-3-Carboxamide ([11C]OMAR)
1 INTRODUCTION
2 SYNTHESIS PROCEDURES
3 QC PROCEDURES
WASTE DISPOSAL INFORMATION
CHEMICAL ABSTRACTS NOMENCLATURE (REGISTRY NUMBER)
REFERENCES AND NOTES
Chapter 9 Synthesis of Carbon-11 Labeled (+)-4-Propyl-3,4,4a,5,6, 10b-Hexahydro-2H-Naphtho[1,2-B][1,4]Oxazin-9-Ol ([11C]-(+)-PHNO)
1 INTRODUCTION
2 SYNTHETIC PROCEDURES
3 QUALITY CONTROL PROCEDURES
WASTE DISPOSAL INFORMATION
CHEMICAL ABSTRACTS NOMENCLATURE (REGISTRY NUMBER)
REFERENCES AND NOTES
Chapter 10 Synthesis of (R)-[N-Methyl-11C]PK11195
1 INTRODUCTION
2 SYNTHESIS PROCEDURES
3 QUALITY CONTROL PROCEDURES
WASTE DISPOSAL INFORMATION
CHEMICAL ABSTRACTS NOMENCLATURE (REGISTRY NUMBER)
REFERENCES AND NOTES
PART III OTHER RADIOPHARMACEUTICALS
Chapter 11 Synthesis of Oxygen-15 Water ([15O]H2O)
1 INTRODUCTION
2 SYNTHESIS PROCEDURES
3 QC PROCEDURES
WASTE DISPOSAL INFORMATION
CHEMICAL ABSTRACTS NOMENCLATURE (REGISTRY NUMBER)
REFERENCES AND NOTES
PART IV NEW METHODS FOR THE SYNTHESIS AND QUALITY CONTROL OF RADIOPHARMACEUTICALS
Chapter 12 Direct, Nucleophilic Radiosynthesis of [18F]Trifluoroethyl Tosylate
1 INTRODUCTION
2 PROCEDURES
3 DISCUSSION
WASTE DISPOSAL INFORMATION
CHEMICAL ABSTRACTS NOMENCLATURE (REGISTRY NUMBER)
References and Notes
Chapter 13 Synthesis of [18F]N-Methyl Lansoprazole via Generation of a [18F]Trifluoromethyl Group
1 INTRODUCTION
2 SYNTHESIS PROCEDURES
3 QUALITY CONTROL PROCEDURES
4 DISCUSSION
WASTE DISPOSAL INFORMATION
CHEMICAL ABSTRACTS NOMENCLATURE (REGISTRY NUMBER)
REFERENCES AND NOTES
Chapter 14 [18F]Fluorination of (Mesityl)(Aryl)Iodonium Salts
1 INTRODUCTION
2 SYNTHESIS PROCEDURES
3 QUALITY CONTROL PROCEDURES
4 DISCUSSION
WASTE DISPOSAL INFORMATION
CHEMICAL ABSTRACTS NOMENCLATURE (REGISTRY NUMBER)
REFERENCES AND NOTES
Chapter 15 Pd(IV)-Mediated Fluorination of Arenes with [18F]F- for PET Imaging
1 INTRODUCTION
2 HISTORY
3 PROCEDURES
4 DISCUSSION
WASTE DISPOSAL INFORMATION
CHEMICAL ABSTRACTS NOMENCLATURE (REGISTRY NUMBER)
REFERENCES AND NOTES
Chapter 16 Silicon Fluoride Acceptors (SiFAs) for Peptide and Protein Labeling with 18F
1 INTRODUCTION
2 PROCEDURES
3 DISCUSSION
WASTE DISPOSAL INFORMATION
CHEMICAL ABSTRACTS NOMENCLATURE
REFERENCES AND NOTES
Chapter 17 Solid Phase Synthesis of [18F]-2-Fluoro-2-Deoxy-d- Glucose: A Resin-Linker-Vector (RLV) Approach
1 INTRODUCTION
2 PROCEDURES
3 DISCUSSION
4 Experimental Supplement
WASTE DISPOSAL INFORMATION
CHEMICAL ABSTRACTS NOMENCLATURE
REFERENCES AND NOTES
Chapter 18 Production and Reaction of [11C]Carbon Disulfide for the Synthesis of [11C]Dithiocarbamates
1 INTRODUCTION
2 PROCEDURES
3 DISCUSSION
ACKNOWLEDGMENTS
WASTE DISPOSAL INFORMATION
CHEMICAL ABSTRACTS NOMENCLATURE (REGISTRY NUMBER)
REFERENCES AND NOTES
Chapter 19 One-Pot, Direct Incorporation of [11CO2] into Carbamates
1 INTRODUCTION
2 PROCEDURES
3 QUALITY CONTROL PROCEDURES
4 DISCUSSION
WASTE DISPOSAL INFORMATION
CHEMICAL ABSTRACTS NOMENCLATURE (REGISTRY NUMBER)
REFERENCES AND NOTES
NOTE
REFERENCES
Chapter 20 Radiosynthesis of [11C]Carboxamides via Reaction of [11C]CO2 Captured by a Cu(I)-Based Catalyst System with Boronic Acid Ester Precursors
1 INTRODUCTION
2 PROCEDURES
3 DISCUSSION
ACKNOWLEDGMENTS
WASTE DISPOSAL INFORMATION
CHEMICAL ABSTRACTS NOMENCLATURE
REFERENCES AND NOTES
NOTES
REFERENCES
Chapter 21 Ethanol as a Solvent for Carbon-11 Radiochemistry
1 INTRODUCTION
2 SYNTHESIS PROCEDURES
3 QC PROCEDURES
WASTE DISPOSAL INFORMATION
CHEMICAL ABSTRACTS NOMENCLATURE (REGISTRY NUMBER)
REFERENCES AND NOTES
Chapter 22 Synthesis and Applications of [11C]Hydrogen Cyanide
1 INTRODUCTION
2 SYNTHESIS PROCEDURES
3 REACTIONS WITH HYDROGEN CYANIDE
WASTE DISPOSAL INFORMATION
CHEMICAL ABSTRACTS NOMENCLATURE (REGISTRY NUMBER)
REFERENCES AND NOTES
Chapter 23 Determination of Radiochemical Purity and Radiochemical Identity of [13N]NH3 Using Thin Layer Chromatography
1 INTRODUCTION
2 PROCEDURES
3 DISCUSSION
4 SUMMARY
WASTE DISPOSAL INFORMATION
CHEMICAL ABSTRACTS NOMENCLATURE (REGISTRY NUMBER)
REFERENCES AND NOTES
Appendix Supplier Information
Index
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