Pyrolysis Mass Spectrometry of Recent and Fossil Biomaterials

Name: Pyrolysis Mass Spectrometry of Recent and Fossil Biomaterials
Brand: Elsevier
Price: 250.0 EUR
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H. L. C. Meuzelaar J. Haverkamp F. D. Hileman(Autor*in)

Elsevier (Verlag)

Erschienen am 1. April 2000

290 Seiten

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Front Cover
Pyrolysis Mass Spectrometry of Recent and Fossil Biomaterials: Compendium and Atlas
Copyright Page
Contents
Abbreviations Used
Preface
Acknowledgements
PART I: COMPENDIUM OF BASIC PRINCIPLES AND APPLICATIONS
CHAPTER 1. ORIGINS AND DEVELOPMENT OF PYROLYSIS MASS SPECTROMETRY OF BIOMATERIALS
1.1. The First Reports
1.2. Direct Probe PY-MS
1.3. Laser PY-MS
1.4. Filament PY-MS
CHAPTER 2. FROM FINGERPRINTING TO STRUCTURAL INVESTIGATION
2.1. Operational Fingerprinting
A New Concept
2.2. Complexity of the Sample
2.3. Additivity of Component Spectra
2.4. Availability of Reference Spectra
2.5. Availability of Standard Reference Materials
2.6. Knowledge of Relevant Pyrolysis Mechanisms
2.7. Availability of Ancillary Analytical Methods
CHAPTER 3. PYROLYSIS MECHANISMS IN BIOMATERIALS
3.1. General Aspects
3.2. Polysaccharides
3.3. Nucleic Acids
3.4. Proteins
3.5. Lipids
3.6. Miscellaneous Biopolymers
CHAPTER 4. THE TECHNIQUE OF CURIE-POINT PYROLYSIS MASS SPECTROMETRY
4.1. Sample Preparation
4.2. Pyrolysis
4.3. Pyrolysate Transfer
4.4. Ionisation
4.5. Mass Analysis
4.6. Ion Detection
4.7. Signal Recording
CHAPTER 5. REPRODUCIBILITY IN CURIE-POINT PYROLYSIS MASS SPECTROMETRY
5.1. Qualitative Reproducibility
5.2. Quantitative Reproducibility
5.3. Factors Influencing Long-Term Reproducibility
5.4. Prospects for Inter-Laboratory Reproducibility
CHAPTER 6. DATA ANALYSIS PROCEDURES
6.1. Available Computer Programs
6.2. Data Pre-Processing
6.3. Univariate Statistical Analysis
6.4. Multivariate Statistical Analysis
6.5. Visualisation Techniques
6.6. Computer-Assisted Chemical Interpretation
6.7. Computer-Assisted Quantitative Analysis of Mixtures
6.8. Future Developments
CHAPTER 7. SELECTED APPLICATIONS TO BIOMATERIALS
7.1. Scope of Analytical Pyrolysis Techniques
7.2. Medical Applications
7.3. Biological Applications
7.4. Environmental Applications
7.5. Biogeochemical Applications
PART II: ATLAS OF SELECTED PYROLYSIS MASS SPECTRA
Contents
CHAPTER 1. INTRODUCTION
1.1. General Remarks
1.2. Sample Preparation
1.3. Analytical Conditions
1.4. Spectrum Presentation Format
1.5. Spectrum Contributions from Inorganic Constituents
1.6. Protein Spectra (Group B)
1.7. Nucleotide and Nucleic Acid Spectra (Group C )
1.8. Lipid Spectra (Group D)
1.9. Spectra of Humic Materials and Geopolymers (Group F)
1.10. Spectra of Other Biochemically Important Compounds (Group G)
CHAPTER 2 . PYROLYSIS MASS SPECTRA
Group A. Carbohydrates and Glycoconjugates
Group B. Peptides and Proteins
Group C. Nucleotides and Nucleic Acids
Group D. Lipids
Group E. Natural Products
Group F. Humic Materials and Geopolymers
Group G. Other Biochemically Important Compounds
Group H. Polymers of Non-Biological Origin
REFERENCES
SUBJECT INDEX

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