Handbook of Laboratory Distillation

Name: Handbook of Laboratory Distillation
Brand: Elsevier
Price: 54.95 EUR
Availability: OnlineOnly

Krell E. Krell(Autor*in)

Elsevier (Verlag)

3. Auflage

Erschienen am 14. Mai 2014

525 Seiten

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978-0-08-087549-1 (ISBN)

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Inhalt

Front Cover
Hand book of Laboratory Distillation
Contents
List of symbols
Chapter 1. Introduction
Chapter 2. A review of the history of laboratory distillation
Chapter 3. Standardization and data on concentrations
3.1 Standardization of distillation appartus
3.2 Definition of concepts
3.3 Symbols and units
3.4 Definitions and conversion of concentrations
Chapter 4. Physical fundamentals of the separation process
4.1 Principles of simple and countercurrent distillation
4.2 Fluid and interface dynamics
4.3 Miscibility of the components
4.4 Vapour pressure-temperature relationship. p - t
4.5 Equation of state and px-diagrams
4.6 Boiling point diagram, epsilon- x, equilibrium curve. y* - x
4.7 Number of theoretical plates (separating stages)
4.8 Theory of packed columns
4.9 Determination of the number of plates and transfer units in the batch and continuous separation of multicomponent mixtures
4.10 Testing plate columns and packed columns
4.11 Pressure drop, limiting velocity and calculation of column dimensions
4.12 Heat calculations
4.13 Distillate properties and distillation diagrams
4.14 Instructions for the calculation of distillation conditions
4.15 Distillation calculations by computer
Chapter 5. Separating processes
5.1 The scale of operation
5.2 Methods of operation
5.3 Temperature
5.4 Distillation pressure
Chapter 6. Selective separating processes
6.1 Carrier vapour distillation
6.2 Azeotropic and extractive distillation
6.3 Solution distillation and special methods
Chapter 7. Constructional materials and apparatus
7.1 Constructional materials for distillation apparatus
7.2 Standard apparatus and unit parts
7.3 Columns
7.4 Condensers and dephlegmators
7.5 Adapters
still and column heads
7.6 Still pots, receivers and fraction collectors
7.7 Insulation and heating devices
7.8 Packings
Chapter 8. Automatic devices, measuring and control equipment
8.1 Automatic equipment
8.2 Temperature measurement and control
8.3 Pressure measurement and control
8.4 Reflux and rate of evaporation
8.5 Measurement of physical data during distillation
8.6 Measurement and metering of gases and liquids
Chapter 9. Arrangement of a distillation laboratory, starting up dietillation apparatus
9.1 Lay-out
9.2 Frameworks and services
9.3 Building up the apparatus
9.4 Sealing ground joints
9.5 Starting up distillation apparatus
9.6 Safety measures
References
Subject index

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