Practical NMR Spectroscopy Laboratory Guide is designed to provide non-expert NMR users, typically graduate students in chemistry, an introduction to various facets of practical solution-state NMR spectroscopy. Each chapter offers a series of hands-on exercises, introducing various NMR concepts and experiments and guiding the reader in running these experiments using an NMR spectrometer. The book is written for use with a Bruker NMR spectrometer running TopSpin software versions 1 or 2. This practical resource functions both as a text for instructors of a practical NMR course and also as a reference for spectrometer administrators or NMR facility directors when doing user training. This guide serves as serve as excellent, practical resource on its own or as a companion book to Timothy Claridge's High-Resolution NMR Techniques in Organic Chemistry, 2nd Edition (Elsevier, 2009).
Sprache
Verlagsort
Verlagsgruppe
Elsevier Science Publishing Co Inc
Zielgruppe
Für Beruf und Forschung
Graduate students in chemistry and related disciplines taking courses in NMR spectroscopy
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Maße
Höhe: 229 mm
Breite: 152 mm
Gewicht
ISBN-13
978-0-12-800689-4 (9780128006894)
Copyright in bibliographic data and cover images is held by Nielsen Book Services Limited or by the publishers or by their respective licensors: all rights reserved.
Schweitzer Klassifikation
Dr. John Simon Harwood has served as Director of the Purdue University Interdepartmental NMR Facility (PINMRF) since 2005, where he has overseen the rationalization and expansion of PINMRF such that the facility now includes two spectrometers with cryoprobes along with an 800-MHz spectrometer. He holds a DSc in Chemistry from the University of Texas at Arlington, and he's held postdoctoral positions at University of Texas Southwestern Medical School and University of California, Berkeley. He is a former manager of the NMR Facility in the Chemistry Department, University of Georgia, and a former director of both the NMR Facilities and the Computational Facility in the Chemistry Department, University of Illinois, Chicago. Dr. Huaping Mo has served as the Associate Director of the Purdue Interdepartmental NMR Facility in the Chemistry Department at Purdue University since 2005. He earned an MSc from Dalian Institute of Chemical Physics, Chinese Academy of Sciences, in 1994 and a PhD from Brandeis University in 1999, where he completed studies on molecular assembly and structures. He conducted his post-doctoral research on protein structures at The Scripps Research Institute. As a researcher at Eli Lilly and Company until 2005, he focused on protein and ligand-protein interaction. His current interests are NMR method development, including methods designed for faraway water suppression and accurate NMR quantitations using either receiving efficiency or large solvent signals. He has authored or co-authored more than 40 publications in peered-reviewed scientific journals.
Autor*in
Purdue University Interdepartmental NMR Facility, Department of Chemistry, Purdue University, West Lafayette, IN, USA
Purdue University Interdepartmental NMR Facility, Department of Chemistry, Purdue University, West Lafayette, IN, USA
Introduction1. Basics and Spectrometer Performance Checks2. Multiple Irradiation and Multiple Pulse Experiments3. Polarization Transfer and Its Applications4. Homonuclear Correlation Experiments5. PFG (Pulsed Field Gradient) Experiments6. Introduction to NMR of Biomolecules in H2O7. Selective Experiments Using Shaped Pulses8. Diffusion Measurements and DOSY (Diffusion Ordered SpectroscopY)
