Alle wichtigen modernen Techniken zur optischen und massenspektrometrischen Elementaranalyse mit Hilfe der Flammen- und Plasmaionisation in einem Buch vereint! Die gründliche Erläuterung der physikalisch-theoretischen und apparativen Grundlagen, Anwendungsbeispiele, einschließlich der konkreten Durchführung der verschiedenen Analysemethoden, und umfangreiche Verweise auf die neueste Literatur ermöglichen auch Neueinsteigern einen problemlosen Zugang zu den vorgestellten Techniken.
Rezensionen / Stimmen
"...summarizes the theory and principles of modern spectrochemical analysis that make use of flames and plasma sources." (SciTech Book News, Vol. 26, No. 2, June 2002) "...provides an excellent theoretical background to the topic..." (Trends in Analytical Chemistry, November 2002)
Auflage
Sprache
Verlagsort
Zielgruppe
Illustrationen
128
20 s/w Tabellen, 128 s/w Abbildungen
illustrations
Maße
Gewicht
ISBN-13
978-3-527-30146-1 (9783527301461)
Schweitzer Klassifikation
Preface.Introduction.1. BASIC PRINCIPLES; Atomic structure; Plasmas; Emission and absorption of radiation; Ionization; Dissociation; Sources for atomic spectrometry; Analytical atomic spectrometry; 2. SPECTROMETRIC INSTRUMENTATION; Figures of merit of an analytical method; Optical spectrometers; Mass spectrometers; Data acquisition and treatment; SAMPLE INTRODUCTION DEVICES; Pneumatic nebulization; Ultrasonic nebulization; Hydride generation; Eletrothermal evaporation; Direct solids sampling; Cathodic sputtering; 4. ATOMIC ABSORPTION SPECTROMETRY; Principles; Atomic absorption spectrometers; Flame atomic absorption; Electrothermal atomic absorption; Hydride generation; Background correction techniques; Fields of application; 5. ATOMIC EMISSION SPECTROMETRY; Principles; Atomic emission spectrometers; Flame emission; Arcs and sparks; Plasma sources; Glow discharges; Laser sources; Fields of application; 6. PLASMA MASS SPECTROMETRY; Principles; Instrumentation; Glow discharge mass spectrometry; ICP mass spectrometry; Fields of application; 7. ATOMIC FLUORESCENCE SPECTROMETRY; Principles; Figures of merit; 8. LASER ENHANCED IONIZATION SPECTROMETRY; Principles; Figues of merit; Analytical Applications.9. SAMPLE PREPARATION FOR ATOMIC SPECTROMETRY; Sample Preparation in direct compact sample analysis.Grinding, sieving and compaction of powders.Sample dissolution.Wet chemical methods.Fusion Procedures.Microwave-assisted methods.Combustion Techniques.Flow injection analysis.Leaching sample preparation methods; 10. COMPARISON WITH OTHER METHODS; Power of detection; Analytical accuracy; Economic aspects.Literature.Index