Ideally suited for second-year undergraduate organic chemistry laboratory courses, this text explains how to perform operations and prepare a variety of organic compounds. As they learn how to filter a hot solution, recrystallize a solid, distil a liquid, perform an extraction and dry a solution, students will come to understand the theory behind the techniques. The book includes substitutions, additions, eliminations and `name' reactions such as the Grignard reaction and the Wittig synthesis as well as procedures for the preparation of interesting compounds such as aspirin and the alarm pheromone of the honey bee.
Auflage
Sprache
Verlagsort
Mill Valley
Großbritannien
Zielgruppe
Für höhere Schule und Studium
Editions-Typ
Produkt-Hinweis
Fadenheftung
Gewebe-Einband
Maße
Höhe: 242 mm
Breite: 198 mm
Dicke: 36 mm
Gewicht
ISBN-13
978-0-935702-76-7 (9780935702767)
Schweitzer Klassifikation
ADDISON AULT is Professor of Chemistry at Cornell College in Mount Vernon, Iowa, where he has taught since 1962.
Safety.- Glassware Used in the Organic Chemistry LabCleaning Up.- Collection and Disposal of Waste.- The Laboratory Notebook.- The Chemical Literature.- Tables.- Filtration.- Recrystallization.- Distillation.- Reduced-Pressure Distillation.- Distillation of Mixtures of Two Immiscible Liquids: Steam Distillation.- Sublimation.- Extraction by Solvents.- Chromatography.- Removal of Water.- Boiling Point.- Melting Point.- Density.- Index of Refraction.- Optical Activity.- Molecular Weight.- Solubility.- Infrared Absorption Spectrometry.- Ultraviolet-Visible Absorption Spectrometry.- Nuclear Magnetic Resonance Spectrometry.- Mass Spectrometry.- Qualitative Tests for the Elements.- Qualitative Characterization Tests: Tests for Functional Groups.- Characterization Through Formation of Derivatives.- Assembling the Apparatus.- Temperature Control.- Methods of Heating and Cooling.- Stirring.- Addition of Reagents.- Control of Evolved Gases.- Concentration.- Use of an Inert Atmosphere.- Working Up the Reaction.
