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This book provides a comprehensive overview of the latest applications of laser-induced breakdown spectroscopy (LIBS) in the environmental and forensic sciences along with chemometric methods. Environmental and forensic science increasingly requires multidisciplinary scientific methods, and LIBS has proven itself a more sensitive and user-friendly technology that can meet the demands of these fields. In addition, LIBS coupled with chemometric modeling approaches creates a powerful tool for detecting and quantitatively predicting the chemical composition of a variety of samples. As a result, this book consolidates essential developments in LIBS, data analysis using chemometrics, and breakthrough applications in environmental and forensic sciences. Beginning with an introduction of the principles of LIBS, the reader is then guided through field and sample-specific applications. An overview of LIBS-Raman instrumentation from basic to more advanced set-ups is also included. The analytical capabilities of the methods in terms of detection limits, accuracy, and precision of measurements for forensic and environmental samples is specifically covered. This book effectively translates the latest developments in algorithms for spectroscopic data and interpretation into these fields. Highlighting the utility of LIBS in environmental and forensic sciences, this book is an essential text for researchers well versed in the fields and as well as readers wanting to familiarize themselves with LIBS as a whole.
Dr. Vivek Kumar Singh joined University of Lucknow, India, in 2021 as an Associate Professor at the Department of Physics. Prior to this, Dr. Singh served at SMVD University, India from July 2008 to December 2021. Dr. Singh has more than 15 years of teaching and research experience at the University level. Dr. Singh completed his D. Phil. degree from University of Allahabad, Prayagraj, Uttar Pradesh, India. In the last decade, Dr. Singh has worked extensively on applications of XRF, LIBS, TOF-SIMS, UV-Visible, and FTIR spectroscopy for the study of several biological specimens such as gallstones, kidney stones, teeth, bones, plants, environmental samples, salts and others. His research interests are in X-ray spectrometry and Laser-induced breakdown spectroscopy. His current research interests include multi-spectroscopy studies of biological samples, organic samples, medicinal plant samples, environmental samples, agricultural samples, and food products. Trace and heavy metal and toxic element determination in bio samples, food products (for quality check), and medicinal plant samples are the major thrust areas of Dr. Singh. He has published more than 100 international research papers, review articles, and book chapters in renowned international journals with good impact factors. He has authored several book chapters in books published by Springer, Elsevier and Wiley. He has successfully edited books on "Nanomaterials and Environmental Biotechnology" published by Springer Nature; "X-Ray Fluorescence in Biological Sciences: Principles, Instrumentations and Applications" published by Wiley & Sons Inc.; and "Laser-Induced Breakdown Spectroscopy (LIBS): Concepts, Instrumentation, Data Analysis and Applications" by Wiley & Sons Inc; and "Applied Raman Spectroscopy" by Elsevier. He is also a life member of several academic and professional societies. Dr. Singh is a recipient of the prestigious "Raman Fellowship" awarded by University Grants Commission (UGC), Govt. of India for the year 2015-16 for Post-Doctoral Research in Lawrence Berkeley National Laboratory (LBNL) operated by University of California, Berkeley, USA. He has been a visiting scientist in many reputed Universities and institutions in USA and delivered lectures at conferences held in USA and China.
Chapter 1: Fundamentals of Laser-Induced Breakdown Spectroscopy and Recent Developments.- Chapter 2: Spatiotemporal Dynamics of Femtosecond Filamentation.- Chapter 3: Tetrahertz Radiation Generation Via Laser-Plasma Interaction.- Chapter 4: Standoff-Laser Induced Breakdown Spectroscopy: Recent Developments and Instrumentation .- Chapter 5: Calibration-Free Laser-Induced Breakdown Spectroscopy: Towards Industrialization.- Chapter 6: Calibration-Free Laser-Induced Breakdown Spectroscopy (CF-LIBS): Capabilities, Limitations and Real-World Applications.- Chapter 7: Sampling Approaches and Optimization in Liquid LIBS Analysis for Environmental Applications.- Chapter 8: Signal Enhancement Techniques in LIBS-Based Experimentations.- Chapter 9: Microwave-Enhanced Laser-Induced Breakdown Spectroscopy.- Chapter 10: Machine Learning in the Context of Laser-Induced Breakdown Spectroscopy.- Chapter 11: Artificial Intelligence Techniques in LIBS Data Analysis and Interpretation.- Chapter 12: Data Processing, Shallow and Deep-Learning Models for LIBS: Basics, Applications and Tools.- Chapter 13: Beyond Peaks and Noise: The Power of Machine Learning in LIBS Analysis.- Chapter 14: Underwater Laser-Induced Breakdown Spectroscopy for Deep-Sea Application.- Chapter 15: LIBS Combined with Machine Learning in Geochemical and Environmental Resources Exploration.- Chapter 16: LIBS-An Emerging Field-Portable Sensor Technology for real-time, in-situ Environmental Analysis.- Chapter 17: Chemometric Tools for the Fast Identification of Microplastics from Environmental Sources.- Chapter 18: Integrating LIBS and Machine Learning: A Dynamic Approach to Plastic Classification in Waste Recycling.- Chapter 19: Laser Induced Breakdown Spectroscopy (LIBS) Sensing for Environmental and Subsurface Monitoring.- Chapter 20: LIBS Application for Monitoring Airborne Particulate Matter and Atmospheric Pollution.- Chapter 21: Enhancement of LIBS Signal under Liquid using External Electric and Magnetic Fields.- Chapter 22: Laser-Induced Breakdown Spectroscopy in Forensic Sensing.- Chapter 23: LIBS Applications in Forensic Dentistry: Predictive Modeling for Sex and Age Determination from Human Tooth.- Chapter 24: Future Development in Laser Induced Breakdown Spectroscopy.
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