Liquid Chromatography Detectors

Name: Liquid Chromatography Detectors
Brand: Elsevier
Price: 230.0 EUR
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Elsevier (Verlag)

Erschienen am 22. September 2011

247 Seiten

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978-0-08-085811-1 (ISBN)

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Inhalt

Front Cover
Liquid Chromatography Detectors
Copyright Page
Contents
Introduction
PART 1: GENERAL CHARACTERISTICS OF LIQUID CHROMATOGRAPHY DETECTORS
Chapter 1. History, function and classification of detectors
History and function
Classification of detectors
References
Chapter 2. Performance criteria of LC detectors
The nature of the detector output
Detector linearity
The determination of the response index of a detector
Detector noise
Detector sensitivity
References
Chapter 3. Detector characteristics that affect column performance
Factors that directly affect band dispersion
Summary
References
Chapter 4. Summary of detector criteria
Chapter 5. Ancillary equipment
Predetector reactors
Noise filters
Integration
References
PART 2: BULK PROPERTY DETECTORS
Chapter 1. General characteristics of bulk property detectors
The limitations of bulk property detectors
General performance characteristics and areas of application
Chapter 2. The refractive index detector
Theory
A commercial example of the refractive index detector
Applications of refractometerdetector
References
Chapter 3. The dielectric constant detector
Theory
References
Chapter 4. The electrical conductivity detector
A commercial example of an electrical conductivity
References
Chapter 5. Additional bulk property detecting systems
The density detector
The thermal conductivity detector
The interferometer detector
The density balance detector
The vapor pressure detector
References
PART 3: SOLUTE PROPERTY DETECTORS
Chapter 1. Principles of detection
Chapter 2. The ultraviolet absorption detector
References
Chapter 3. The fluorometric detector
References
Chapter 4. The polarographic detector
References
Chapter 5. The heat of adsorption detector
References
Chapter 6. The spray impact detector
References
Chapter 7. The radioactivity detector
References
Chapter 8. The electron capture detector
References
Chapter 9. Transport detectors
References
PART 4: THE USE OF DETECTORS IN LIQUID CHROMATOGRAPHY
Chapter 1. The selection of the appropriate detector
The UV detector
The refractive index detector
The fluorescence detector
The wire transport detector
The electron capture detector
The electrical conductivity detector
References
Chapter 2. Quantitative and qualitative analysis
Column temperature
Sample load
Manual measurement of chromatographic data
Computer data processing
Qualitative analysis
Quantitative analysis
References
Chapter 3. Practical hints on detector operation
The recorder
The amplifier
Detector cells
Bubbles - their removal and prevention
Spurious peaks
Base line instability
The moving wire detector
The conductivity detector
The refractive index detector
Chapter 4. Special detector techniques
The differential detector
The integral detector
Vacancy chromatography
References
Chapter 5. Spectroscopic detectors
The LC/UV combination
The Variscan LC/UVspectrometer system
The LC/MS combination
LC/MS by direct sampling of column eluent
The wire transport LC/MS system
The Finnigan LC/MS transport system
References
Index

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