Ion Chromatography

Name: Ion Chromatography
Brand: Elsevier
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Elsevier (Verlag)

Erschienen am 16. Juli 1990

775 Seiten

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Inhalt

Front Cover
Ion Chromatography: Principles and Applications
Preface
Short Contents
Full Contents
Chapter 1. Introduction
1.1 BACKGROUND TO ION CHROMATOGRAPHY
1.2 WHAT IS ION CHROMATOGRAPHY?
1.3 ORGANIZATION OF THIS BOOK
1.4 SOME FUNDAMENTAL CHROMATOGRAPHIC CONCEPTS
1.5 REFERENCES
PART I: ION-EXCHANGE SEPARATION METHODS
Chapter 2 An Introduction to Ion-Exchange Methods
2.1 INTRODUCTION TO ION-EXCHANGE
2.2 CLASSIFICATION OF ION CHROMATOGRAPHIC METHODS EMPLOYING ION-EXCHANGE SEPARATION
2.3 REFERENCES
Chapter 3 Ion-Exchange Stationary Phases for Ion Chromatography
3.1 INTRODUCTION
3.2 SILICA-BASED ION-EXCHANGE MATERIALS
3.3 RESIN-BASED ION-EXCHANGERS
3.4 AGGLOMERATED ION-EXCHANGE RESINS
3.5 HYDROUS OXIDE ION-EXCHANGERS
3.6 SIMULTANEOUS SEPARATION OF ANIONS AND CATIONS
3.7 REFERENCES
Chapfer 4 Eluents for Ion-Exchange Separations
4.1 INTRODUCTION
4.2 ELUENT CHARACTERISTICS
4.3 ELUENTS FOR NON-SUPPRESSED ION CHROMATOGRAPHY
4.4 ELUENTS FOR SUPPRESSED ION CHROMATOGRAPHY
4.5 GRADIENT ELUTION IN ION-EXCHANGE SEPARATIONS
4.6 EXTRANEOUS (SYSTEM) PEAKS IN ION-EXCHANGE IC
4.7 REFERENCES
Chapter 5 Retention Models f o r Ion-Exchange
5.1 INTRODUCTlON
5.2 RETENTION MODELS FOR ANION-EXCHANGE
5.3 RETENTION MODELS FOR CATION-EXCHANGE
5.4 REFERENCES
PART II ION-INTERACTION, ION-EXCLUSION AND MISCELLANEOUS SEPARATION METHODS
Chapter 6 Ion-Interaction Chromatography
6.1 INTRODUCTlON
6.2 MECHANISM
6.3 STATIONARY PHASES AND ELUENTS
6.4 RETENTION MODELS FOR DYNAMIC COATING ION-INTERACTION CHROMATOGRAPHY
6.5 APPLICATIONS
6.6 REFERENCES
Chapter 7 Ion-Exclusion Chromatography
7.1 INTRODUCTlON
7.2 STATIONARY PHASES
7.3 ELUENTS
7.4 FACTORS INFLUENCING RETENTION IN ION-EXCLUSION CHROMATOGRAPHY
7.5 RETENTION MODEL FOR ION-EXCLUSION CHROMATOGRAPHY
7.6 APPLICATIONS OF ION-EXCLUSION CHROMATOGRAPHY
7.7 REFERENCES
Chapter 8 Miscellaneous Separation Methods
8.1 INTRODUCTION
8.2 REVERSED-PHASE LIQUID CHROMATOGRAPHY
8.3 CHELATING STATIONARY PHASES
8.4 MICELLE EXCLUSION CHROMATOGRAPHY
8.5 REFERENCES
PART III DETECTION METHODS
Chapter 9 Conductivity Detection
9.1 INTRODUCTION
9.2 PRINCIPLES OF CONDUCTIVITY DETECTION
9.3 MODES OF CONDUCTIVITY DETECTION
9.4 ELECTRONIC CIRCUITRY AND CELL DESIGN FOR CONDUCTIVITY DETECTION
9.5 SUPPRESSORS IN IC
9.6 PERFORMANCE CHARACTERISTICS OF CONDUCTIVITY DETECTORS
9.7 APPLICATIONS OF CONDUCTIVITY DETECTION IN IC
9.8 REFERENCES
Chapter 10 Electrochemical Detection (Amperometry, Voltammetry and Coulometry)
10.1 INTRODUCTlON
10.2 MODES OF OPERATION OF ELECTROCHEMICAL DETECTORS
10.3 ELECTRODES FOR AMPEROMETRIC DETECTION
10.4 FLOW-CELL DESIGN AND RESPONSE EQUATIONS
10.5 APPLICATIONS OF ELECTROCHEMICAL DETECTION
10.6 REFERENCES
Chapter 11 Potentiometric Detection
1 1.1 INTRODUCTION
1 1.2 PRINCIPLES OF POTENTIOMETRIC DETECTION
1 1.3 INDICATOR ELECTRODES AND RESPONSE PROFILES
1 1.4 FLOW-CELLS FOR POTENTIOMETRIC DETECTION
1 1.5 APPLICATIONS OF POTENTIOMETRIC DETECTION IN IC
11.6 REFERENCES
Chapter 12 Spectroscopic Detection Methods
12.1 INTRODUCTION
12.2 UV-VISIBLE SPECTROPHOTOMETRIC DETECTION IN IC METHODS USING ION-EXCHANGE SEPARATIONS
12.3 SPECTROPHOTOMETRIC DETECTION IN IC METHODS USING ION-INTERACTION SEPARATIONS
12.4 SPECTROPHOTOMETRIC DETECTION IN IC METHODS USING ION-EXCLUSION SEPARATIONS
12.5 REFRACTIVE INDEX DEECTION
12.6 PHOTOLUMINESCENCE DETECTION IN IC
12.7 ATOMIC SPECTROSCOPIC DETECTION IN IC
12.8 REFERENCES
Chapter 13 Detection by Post-Column Reaction
1 3.1 INTRODUCTION
13.2 HARDWARE FOR POST-COLUMN REACTTON
13.3 PCR DETECTION OF INORGANIC ANIONS
13.4 PCR DETECTION OF INORGANIC CATIONS
13.5 PCR DETECTION OF ORGANIC SPECIES
13.6 REFERENCES
PART IV PRACTICAL ASPECTS
Chapter 14 Sample Handling in Ion Chromatography
14.1 INTRODUCTION
14.2 SAMPLE COLLECTION PROCEDURES
14.3 EXTRACTION OF IONIC SPECIES FROM SAMPLES
14.4 SAMPLE CLEANUP METHODS
14.5 CONTAMINATION EFFECTS
14.6 SAMPLE HANDLING FOR ULTRA-TRACE ANALYSIS
14.7 MATRIX ELIMINATION METHODS
14.8 REFERENCES
Chapter 15 Methods Development
15.1 INTRODUCTION
15.2 SELECTION OF APPROPRIATE CHROMATOGRAPHIC PARAMETERS
15.3 OPTlMlZATION OF THE ELUENT COMPOSITION
15.4 MULTI-DIMENSIONAL (COUPLED) IC METHODS
15.5 AUTOMATION IN IC
1 5.6 REFERENCES
PART V APPLICATIONS OF ION CHROMATOGRAPHY
Overview of the Applications Section
Chapter 16 Environmental Applications
16.1 OVERVIEW
16.2 REFERENCES
Chapter 17 Industrial Applications
17.1 OVERVIEW
17.2 REFERENCES
Chapter 18 Analysis of Foods and Plants
18.1 OVERVIEW
18.2 REFERENCES
Chapter 19 Clinical and Pharmaceutical Applications
19.1 OVERVIEW
19.2 REFERENCES
Chapter 20 Analysis of Metals and Metallurgical Solutions
20.1 OVERVIEW
20.2 REFERENCES
Chapter 21 Analysis of Treated Waters
21.1 OVERVIEW
21.2 REFERENCES
Chapter 22 Miscellaneous Applications
22.1 OVERVIEW
22.2 REFERENCES
Appendix A. Statistical Information on Ion Chromatography Publications
Appendix B. Abbreviations and Symbols
Index
Journal of Chromatography Library (other volumes in the Series )

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