Chromatography and Separation Science

Name: Chromatography and Separation Science
Brand: Academic Press
Price: 124.0 EUR
Availability: OnlineOnly

Satinder Ahuja(Autor*in)

Academic Press

Erschienen am 11. Januar 2003

262 Seiten

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978-0-08-050112-3 (ISBN)

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Inhalt

Cover
Contents
Preface
Chapter 1. Relating Chromatography to Separations
I. Defining Separation
II. Evolution of Chromatography
III. Separations in Everyday Life
IV. Basis of Separations
V. Modes of Chromatography
VI. Unified Separation Science
VII. Selectivity and Detectability
References
Questions for Review
Chapter 2. Simple Separation Methods
I. Evaporation
II. Precipitation
III. Crystallization
IV. Filtration
V. Membrane Separations
VI. Distillation
VII. Extraction
References
Questions for Review
Chapter 3. Equilibrium Processes in Separations
I. Molecular Interactions
II. Separation Thermodynamics
References
Questions for Review
Chapter 4. The Molecular Basis of Separation
I. Molecular Interactions
II. Solubility Parameter Theory
III. Group Interactions
References
Questions for Review
Chapter 5. MassTransport and Separation
I. Types of Diffusion
II. Modeling Diffusion
III. Chromatographic Implications
IV. Diffusion Rates in Various Media
V. Mass Transfer
References
Questions for Review
Chapter 6. Chromatographic Methods
I. General Classification of Chromatographic Methods
II. Classification Based on Retention Mode
III. Classification Based on Sample Introduction
IV. Separation Characteristics of Chromatographic Methods
V. Basic Chromatographic Theory
References
Questions for Review
Chapter 7. Paper Chromatography
I. Chromatography Paper
II. Sample Preparation
III. Sample Cleanup
IV. Derivatization
V. Mobile Phases and Stationary Phases
VI. Development of Chromatograms
VII. Detection
VIII. Quantitation
References
Questions for Review
Chapter 8. Thin-Layer Chromatography
I. Stationary Phases for TLC
II. TLC of Enantiomeric Compounds
III. Sample Application
IV. Mobile Phases
V. Development of Chromatograms
VI. Detection and Quantitation
VII. Applications
References
Questions for Review
Chapter 9. Gas Chromatography
I. Equipment
II. Separation Process
III. Columns
IV. Gas Chromatographic Detectors
V. Recording and Analysis
VI. Resolution
VII. Selection of a Stationary Phase
References
Questions for Review
Chapter 10. High-Pressure Liquid Chromatography
I. Evolution of HPLC
II. Advantages over Gas Chromatography (GC)
III. Separation Process
IV. Retention Parameters in HPLC
V. Resolution and Retention Time
VI. Equipment
VII. Separation Mechanism in HPLC
VIII. Stationary Phase Effects
IX. A Case Study of Retention Mechanism Investigations
X. Molecular Probes/Retention Index
XI. Mobile Phase Selection and Optimization
References
Questions for Review
Chapter 11. Evolving Methods and Method Selection
I. Evolving Methodologies
II. Selection of a Separation Method
III. Chiral Separations
IV. Comparison of GC, SFC, HPLC, and CEC for a Selective Separation
References
Questions for Review
Index

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