Is there any iron in moon dust? How much aspirin is there in a headache tablet? What trace metals are there in a tin of tuna? What is the purity and chemical structure of a newly prepared compound? The answers may be given by a simple chemical test or by the use of costly and complex instrumentation.
Principles and Practice of Analytical Chemistry provides a basic understanding of the principles, instrumentation, and applications of chemical analysis. The presentation is designed to aid rapid assimilation by emphasizing unifying themes common to groups of techniques and by including short summaries at the beginning of each section. The book gives substantial coverage to high-performance capillary electrophoresis, two-dimensional nuclear magnetic resonance spectrometry, software for instrument control and real-time data control, and the use of laboratory information management systems.
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978-0-7487-5163-1 (9780748751631)
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Schweitzer Klassifikation
INTRODUCTION
The Scope of Analytical Chemistry
The Function of Analytical Chemistry
Analytical Problems and Their Solution
The Nature of Analytical Methods
Trends in Analytical Methods and Procedures
Glossary of Terms
THE ASSESSMENT OF ANALYTICAL DATA
Definitions and Basic Concepts
The Nature and Origin Errors
The Evaluation of Results and Methods
PH, COMPLEXATION AND SOLUBILITY EQUILIBRIA
Chemical Reactions in Solution
Solvents in Analytical Chemistry
Add-Based Equilibria
Complexation Equilibria
Solubility Equilibria
SEPARATION TECHNIQUES
Solvent Extraction
Chromatography
Electrophoresis
Titrimetry and Gravimetry
Titrimetry
Gravimetry
ELECTROCHEMICAL TECHNIQUES
Potentiometry
Polarography, Stripping Voltammetry and Amperometric Techniques
Electrogravity and Coulometry
Conductometric Titrations
AN INTRODUCTION TO ANALYTICAL SPECTROMETRY
Electromagnetic Radiation
Atomic and Molecular Energy
The Absorption and Emission of Electromagnetic Radiation
The Complexity of Spectra and the Intensity of Spectral Lines
Analytical Spectrometry
Instrumentation
ATOMIC SPECTROMETRY
Arc/Spark Atomic (Optical) Emission Spectrometry
Glow Discharge Atomic Emission Spectrometry
Plasma Emission Spectrometry
Inductively Coupled Plasma-Mass Spectrometry (ICP-MS)
Flame Emission Spectrometry
Atomic Absorption Spectrometry
X-Ray Emission Spectrometry
MOLECULAR SPECTROMETRY
Visible and Ultraviolet Spectrometry
Infrared Spectrometry
Nuclear Magnetic Resonance Spectrometry (NMR)
Mass Spectrometry
RADIOCHEMICAL METHODS IN ANALYSIS
Nuclear Structure and Nuclear Reactions
Instrumentation and Measurement of Radioactivity
Analytical Uses of Radionucleides
THERMAL TECHNIQUES
Thermogravimetry
Differential Thermal Analysis
Differential Scanning Calorimetry
Thermomechanical Analysis (TMA) and Dynamic Mechanical Analysis (DMA)
Pyrolysis - Gas Chromatography
OVERALL ANALYTICAL PROCEDURES AND THEIR AUTOMATION
Sampling and Sample Pretreatment
Examples of Analytical Problems and Procedures
The Automation of Analytical Procedures
THE ROLE OF COMPUTERS AND MICRO-PROCESSORS IN ANALYTICAL CHEMISTRY
Introduction
Computers and Microprocessors
Instrument-Computer Interfaces
The Scope of Microprocessor Control and Computers in Analytical Laboratories
Index
