Today, we all know that the combination of a conventional injection procedure, a single analytical column and a selective detector often does not suffice to recognize and quantify all analytes of interest in a sample. During the eighties, the use of multidimensional approaches slowly began to make headway to help solve the many, and often complex, problems concerning the provisional identification, or confirmation of the presence, of analytes of interest, the design of separation systems with a considerably improved separation efficiency, and the generally felt need to incorporate the sample preparation in the total analytical procedure. Two major branches emerged - hyphenation, which is often defined as the on-line combination of a separation technique and a spectroscopic detection device which provides structural information, and coupled-column techniques.Sometimes hyphenation is used to describe both of these branches, a practice that has also been followed when selecting the title of the present volume. Gradually the glamour of hyphenation began to be recognised, and the hype and fascination were born.
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Verlagsort
Verlagsgruppe
Elsevier Science & Technology
Zielgruppe
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ISBN-13
978-0-444-50190-5 (9780444501905)
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Schweitzer Klassifikation
Autor*in
Department of Analytical Chemistry, Free University Amsterdam, The Netherlands
Selected papers: Preface (U.A.Th. Brinkman). Solid-phase extraction: method development, sorbents, and coupling with liquid chromatography (M.-C. Hennion). Membrane-based sample preparation coupled on-line to chromatography or electrophoresis (N.C. van de Merbel). Supercritical fluids in separation science - the dreams, the reality and the future (R.M. Smith). Recent developments in microcolumn liquid chromatography (J.P.C. Vissers). Developments in sample preparation and separation techniques for the determination of inorganic ions by ion chromatography and capillary electrophoresis (P.R. Haddad et al.). State-of-the-art in liquid chromatography-mass spectrometry (W.M.A. Niessen). Liquid chromatography-nuclear magnetic resonance spectroscopy (K. Albert). Liquid chromatography-Fourier-transform infrared spectrometry (G.W. Somsen et al.). Liquid chromatography-inductively coupled plasma mass spectrometry (K.L. Sutton, J.A. Caruso). Programmed temperature vaporiser-based injection in capillary gas chromatography (W. Engewald et al.). On-line combination of aqueous-sample preparation and capillary gas chromatography (J.J. Vreuls et al.). High-speed gas chromatography: an overview of various concepts (C.A. Cramers et al.). Gas chromatography with spectroscopic detectors (N. Ragunathan et al.). Planar chromatography at the turn of the century (C.F. Poole). The state of the art in thin-layer chromatography-mass spectrometry: a critical appraisal (I.D. Wilson). Overview of capillary electrophoresis and capillary electrochromatography (K.D. Altria). Electrokinetic chromatography (J.P. Quirino, S. Terabe). Coupling of biological sample handling and capillary electrophoresis (J.R. Veraart et al.). Analysis of DNA adducts using high-performance separation techniques coupled to electrospray ionization mass spectrometry (C.L. Andrews et al.). Author index. Subject index.