In-Situ Transmission Electron Microscopy Experiments
Design and Practice
1st Edition
Published on 9. May 2023
384 pages
978-3-527-83483-9 (ISBN)
Description
A comprehensive guide to planning and performing in situ TEM measurements that explains the basic principles and current approaches for in situ/operando measurements of material morphology, structure and chemical changes under different kinds of stimuli. Written for practitioners, it addresses experimental limitations and shows how to overcome them, explains how work with and enhance commercially available equipment, and discusses future perspectives in the field. Throughout, the reader will find practical advice and hands-on knowledge from the author's life-long efforts in extending the boundaries of this novel technology.
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Person
Renu Sharma received a B.S. and B.Ed. in Physics and Chemistry from Panjab University, India, and M.S. and Ph.D. degrees in Solid State Chemistry from the University of Stockholm, Sweden. She is currently a NIST Emeritus Fellow after working there as a project leader from 2009 to 2019. She came to NIST from Arizona State University (ASU), where she began as a Faculty Research Associate in the Department of Chemistry and Biochemistry and the Center for Solid State Science, served as a Senior Research Scientist in the LeRoy Eyring Center for Solid State Science and as an affiliated faculty member of the School of Materials and Department of Chemical Engineering. Dr. Sharma is one of the pioneers in the development of environment cell scanning/transmission electron microscopy (E(S)TEM), combining atomic-scale resolution with dynamic chemical analysis of gas-solid reactions. She has applied this powerful technique to characterize atomic-scale mechanisms underlying the synthesis and reactivity of nanoparticles (including catalysts), nanotubes, nanowires, inorganic solids, ceramics, semiconductors, and superconductor materials. She has over 180 publications to her name.
Content
IN-SITU TEM
General Scope of the Book and Review of the Chapters
Why in-situ TEM?
TEM Overview
TEM/STEM-Based Characterization Techniques
Other Techniques
Introduction to Different Stimuli Used for In situ TEM
EXPERIMENT DESIGN PHILOSOPHY
General Aspects
Choice of Technique and the Microscope
TEM Holder Design and Selection
Specimen Design and Preparation
Guidelines for Experimental Setup
Practical Example of Designing In-situ TEM Experiments
Applications to Quantitative Data
IN-SITU HEATING
History
Currently Available Heating Holders
Experimental Considerations
Select Applications
Limiations and Possibilities
IN SITU CRYO-TEM
Historical Perspective
Specimen Holder Design and Function
Specimen Design and Preparation
Practical Aspects of Performing Cryogenic Cooling
Some Noteworthy Applications
DESIGNING LIQUID AND GAS CELL HOLDERS
Historical Perspective
Design Philosophy
Windows
Microfabricated Window-Cell (Microchips)
Examples of Modified Window Holders
IN SITU SOLID-LIQUID INTERACTIONS
Historical Perspective
Holder Design and Selection
Specimen Design and Preparation
Data Acquisition
Practical Challenges
Select Examples of Applications
IN-SITU GAS-SOLID INTERACTIONS
Historical Perspective
Current Strategies
Gas Manifold Design and Construction
Practical Aspects of Performi Experiment in Gas Environments
Select Examples of Applications
Review of Benefits and Limitations
MULTIMODAL AND CORRELATIVE MICROSCOPY
Multimodal TEM
Correlative Approaches
DATA PROCESSING AND MACHINE LEARNING
History of Image Simulation and Processing
Current Status
Data Management
Data Processing and Machine Learning (ML)
Select Applications
Future Needs
Limitations
FUTURE VISION
Historical Aspects
Current Status
Technical Challenges
Developing Relevant Strategies
General Scope of the Book and Review of the Chapters
Why in-situ TEM?
TEM Overview
TEM/STEM-Based Characterization Techniques
Other Techniques
Introduction to Different Stimuli Used for In situ TEM
EXPERIMENT DESIGN PHILOSOPHY
General Aspects
Choice of Technique and the Microscope
TEM Holder Design and Selection
Specimen Design and Preparation
Guidelines for Experimental Setup
Practical Example of Designing In-situ TEM Experiments
Applications to Quantitative Data
IN-SITU HEATING
History
Currently Available Heating Holders
Experimental Considerations
Select Applications
Limiations and Possibilities
IN SITU CRYO-TEM
Historical Perspective
Specimen Holder Design and Function
Specimen Design and Preparation
Practical Aspects of Performing Cryogenic Cooling
Some Noteworthy Applications
DESIGNING LIQUID AND GAS CELL HOLDERS
Historical Perspective
Design Philosophy
Windows
Microfabricated Window-Cell (Microchips)
Examples of Modified Window Holders
IN SITU SOLID-LIQUID INTERACTIONS
Historical Perspective
Holder Design and Selection
Specimen Design and Preparation
Data Acquisition
Practical Challenges
Select Examples of Applications
IN-SITU GAS-SOLID INTERACTIONS
Historical Perspective
Current Strategies
Gas Manifold Design and Construction
Practical Aspects of Performi Experiment in Gas Environments
Select Examples of Applications
Review of Benefits and Limitations
MULTIMODAL AND CORRELATIVE MICROSCOPY
Multimodal TEM
Correlative Approaches
DATA PROCESSING AND MACHINE LEARNING
History of Image Simulation and Processing
Current Status
Data Management
Data Processing and Machine Learning (ML)
Select Applications
Future Needs
Limitations
FUTURE VISION
Historical Aspects
Current Status
Technical Challenges
Developing Relevant Strategies
