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Systematic Materials Analysis, Volume III presents brief discussions on a broad range of instrumental methods and approaches that will yield the desired information about a given material. The book discusses the selection of analytical methods on the bases of specimen limitations and information desired. The chapters on specific instruments briefly outline the theories of operation and describe the capability of the methods for qualitative and quantitative measurements of chemical composition, structure, and texture (as applicable). The commercial instruments and techniques discussed include arc, spark, laser, plasmas, flame photometry, gas analysis techniques, combustion methods, gas chromatography, and ion-scattering spectrometry. The Mossbauer spectrometry; optical microscopy; x-ray diffraction; x-ray fluorescence; and absorption spectrometry are also encompassed. Materials analyst, materials scientist, chemists, and engineers will find the book invaluable.
Language
Place of publication
Publishing group
Elsevier Science & Techn.
ISBN-13
978-1-4832-1982-0 (9781483219820)
Schweitzer Classification
Preface AcknowledgmentsContents of Other Volumes Chapter 20 Computer-Instrument Interfacing Introduction 1 Theory 2 Quantitative Interface Characteristics 3 The Interface Specification 4 Interface Implementation 5 Software Techniques 6 Conclusion and Trends References Chapter 21 Emission Spectrometry: Arc, Spark, Laser, and Plasmas Introduction 1 Theory 2 Instrumentation 3 Applications of Emission Spectrometry References Chapter 22 Flame Photometry Introduction 1 Fundamentals 2 The Flame 3 Instrumentation 4 Interference 5 Analytical Characteristics of Flame Photometry 6 Analytical Methodology 7 Applications References Chapter 23 Gas Analysis Techniques and Combustion Methods Introduction 1 Gas Analysis 2 Combustion Methods for Elemental Analysis References Bibliography Chapter 24 Gas Chromatography Introduction 1 Theory 2 Gas Chromatography Apparatus 3 Data Form 4 Applications and Limitations 5 Auxiliary Techniques 6 Special Literature on Gas Chromatography References Selected Additional Reading Chapter 25 Ion-Scattering Spectrometry for Surface Analysis Introduction 1 Theory 2 Experimental Technique and Apparatus 3 Applications 4 Conclusion References Chapter 26 Mössbauer Spectrometry Introduction 1 Theory 2 Instrumentation 3 Sample Preparation 4 Applications 5 Data Processing References Chapter 27 Optical Microscopy Introduction 1 Optical Microscopes 2 Use of Optical Microscope for Identification of Crystalline Phases 3 Use of Optical Microscope for Detection of Crystal Imperfections 4 Use of Optical Microscope in Chemical Analysis 5 Use of Optical Microscope in Textural Analysis References Chapter 28 X-Ray Diffraction Introduction 1 The Crystalline State 2 X-Ray Diffraction Processes 3 Preliminary Discussion of Powder and Single-Crystal Patterns, and Their, Information Content 4 The Production and Monochromatization of X-Ray for Diffraction 5 The Use of X-Ray Diffraction for the Analysis of Materials 6 Methods for Recording Diffraction Patterns of Materials 7 Additional Uses of X-Ray Diffraction Data 8 Structure Determination 9 Crystallography by Diffraction of Radiation Other Than X-Ray References Chapter 29 X-Ray Fluorescence and Absorption Spectrometry Introduction 1 Essentials of X-Ray Fluorescence Spectrometry 2 Essentials of X-Ray Absorption Analysis 3 Instrumentation 4 Literature 5 Applications 6 Data Form and Interpretation 7 Accessories and User Modifications References Author Index Subject Index