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Systematic Materials Analysis, Volume IV presents refined instrumental methods available for materials analysis, which involves the complete characterization of a material, including structural and textural analyses in addition to chemical analysis. This volume is composed of 11 chapters. Each chapter on specific instruments outlines the theories of operation and describes their capability for qualitative and quantitative measurements of chemical composition, structure, and texture. The sensitivity and selectivity of each method are emphasized. The specific techniques and instruments covered in this book include the atomic-absorption and atomic-fluorescence flame photometry, ion microprobe, mass spectrometry, neutron diffractometry, polarimetry, polarography, dynamic thermal analysis, and transmission electron microscopy. This book is intended primarily to materials analysts, engineers, researchers, and undergraduate and graduate level students.
Language
Place of publication
Publishing group
Elsevier Science & Techn.
ISBN-13
978-0-323-14756-9 (9780323147569)
Schweitzer Classification
List of ContributorsPrefaceAcknowledgmentsContents of Other VolumesChapter 30 Atomic-Absorption and Atomic-Fluorescence Flame Photometry Introduction 1 Fundamentals 2 The Flame 3 Instrumentation 4 Interferences 5 Analytical Characteristics 6 Analytical Methodology 7 Applications ReferencesChapter 31 Ion Microprobe 1 Ion Sputtering as an Analytical Tool 2 Ion Microprobe Instrumentation 3 Experimental Procedures 4 Quantitative Analysis ReferencesChapter 32 Mass Spectrometry Introduction 1 Ion Sources 2 Mass Analyzers 3 Detectors 4 Inlet Systems 5 Computers BibliographyChapter 33 Molecular Weight Determinations Introduction 1 Theory 2 Molecular Weight Distribution 3 Methods for Determining Molecular Weight ReferencesChapter 34 Neutron Diffractometry Introduction 1 Theory and Comparison with Other Diffraction Techniques 2 Instrumentation 3 Applications 4 Other Types of Investigations 5 Future of Neutron Scattering ReferencesChapter 35 Particulate Characterization Introduction 1 Particle Size Analysis 2 Surface Area Analysis 3 Powder Density ReferencesChapter 36 Polarimetry Introduction 1 Theory 2 Instrumentation 3 Applications ReferencesChapter 37 Polarography and Related Methods Introduction to Electrochemical Methods of Analysis 1 Theory of Polarography and Related Methods 2 Applications and Limitations 3 Data Form ReferencesChapter 38 Methods for the Detection of Noncentrosymmetry in Solids Introduction 1 Symmetry Elements and Methods for Their Determination 2 Second Harmonic Generation in Crystals and Powders 3 Design and Operation of a Second Harmonic Analyzer 4 Application to Specific Problems ReferencesChapter 39 Dynamic Thermal Analysis Introduction 1 Thermogravimetry 2 Differential Thermal Analysis and Differential Scanning Calorimetry 3 Thermomechanical Analysis 4 Conclusion ReferencesChapter 40 Transmission Electron Microscopy Introduction 1 A Description of the Electron Microscope and Its Capabilities 2 Replica Techniques 3 Preparation of Thin Foils 4 Image Contrast in Thin Foils 5 Applications of Thin Foil Techniques ReferencesAuthor IndexSubject Index