
Chemical Derivatization in Gas Chromatography
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Content
- Front Cover
- Chemical Derivatization in Gas Chromatography
- Copyright Page
- Contents
- Abbreviations used
- Preface
- Introduction
- Chapter 1. Reasons for using chemical derivatives in gas chromatography
- 1.1. Volatility of sample compounds
- 1.2. Spurious adsorption
- 1.3. Separation of closely related compounds
- 1.4. Selective and sensitive detection
- 1.5. Identification
- References
- Chapter 2. Sample preparation and derivatization techniques
- 2.1. Sampling techniques
- 2.2. Sample treatment prior to analysis
- 2.3. Preparation of derivatives
- 2.4. Gas chromatography
- References
- Chapter 3. Identification and quantitation
- 3.1. Identification
- 3.2. Quantitation
- References
- Chapter 4. Most frequent derivatives and methods for their preparation
- 4.1. Esters
- 4.2. Ethers
- 4.3. Acyl derivatives
- 4.4. Silyl derivatives
- 4.5. Oximes and hydrazones
- 4.6. Cyclic derivatives
- References
- Chapter 5. Derivatization of individual species of compounds
- 5.1. Alcohols and phenols
- 5.2. Aldehydes and ketones
- 5.3. Amines
- 5.4. Sulphur compounds
- 5.5. Carboxylic acids
- 5.6. Amino acids
- 5.7. Thyroid hormones
- 5.8. Steroids
- 5.9. Sugars and related compounds
- 5.10. Bases of nucleic acids, nucleosides and nucleotides
- 5.11. Insecticides and other pesticides
- 5.12. Pharmaceuticals and drugs
- 5.13. Anions of mineral acids
- 5.14. Cations of metals
- 5.15. Miscellaneous
- References
- Appendix 1. Purification of chemicals and solvents
- Appendix 2. A list of some suppliers of reagents and accessoires for derivatization
- Subject index
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