Quantitative Column Liquid Chromatography
A Survey of Chemometric Methods
Published on 14. May 2014
314 pages
978-0-08-085832-6 (ISBN)
Description
Quantitative Column Liquid Chromatography
More details
Series
Language
English
Place of publication
Burlington
Netherlands
Product notice
Windows
ISBN-13
978-0-08-085832-6 (9780080858326)
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Schweitzer Classification
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04/2000
Elsevier
€235.22
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Content
- Front Cover
- Quantitative Column Liquid Chromatography: A Survey of Chemometric Methods
- Copyright Page
- Contents
- Journal of Chromatography Library
- Preface
- CHAPTER 1. ORGANIZATION
- 1.1 Introduction
- 1.2 Functional Classification of Quantitative Methods
- 1.3 Separation Mechanism
- 1.4 Solute Properties
- 1.5 Chromatogram Components
- 1.6 Preview
- 1.7 References
- CHAPTER 2. CHEMOMETRICS IN COLUMN LIQUID CHROMATOGRAPHY
- 2.1 Introduction
- 2.2 Regression
- 2.3 Implementing Non-Linear Regression
- 2.4 Error Propagation
- 2.5 Statistical Experimental Design
- 2.6 Factor Analysis
- 2.7 Pattern Recognition
- 2.8 Conclusions: Chemometrics in LC
- 2.9 References
- CHAPTER 3. FRACTIONATION
- 3.1 Introduction
- 3.2 Defining Acceptable Fractionation
- 3.3 Mechanisms of Separation
- 3.4 Predicting Fractionation
- 3.5 Selection of the Chromatographic Mode
- 3.6 Isocratic Liquid Chromatography
- 3.7 Gradient Column Liquid Chromatography
- 3.8 Conclusions: Fractionation
- 3.9 References
- CHAPTER 4. DETECTION
- 4.1 Single-Channel Detectors
- 4.2 Multiple Single-Channel Photometric Detectors
- 4.3 Rapid Scan Spectrophotometers
- 4.4 Molecular Weight Identification in SEC
- 4.5 Conclusions: Detection
- 4.6 References
- CHAPTER 5. CALIBRATION
- 5.1 Introduction
- 5.2 Calibration with Single-Solute Standards
- 5.3 Calibration with Multi-Solute Standards
- 5.4 The Quantitative Influence of System Conditions on Calibration Curves
- 5.5 Conclusions: Calibration
- 5.6 References
- CHAPTER 6. RESOLUTION CORRECTION
- 6.1 Introduction
- 6.2 Geometric Constructions
- 6.3 Curve Fitting
- 6.4 Accumulated Detector Response
- 6.5 Deconvolution
- 6.6 Correcting Molecular Weight Averages
- 6.7 Calibration Curve Search
- 6.8 New Polymer Detectors and Complex Polymers
- 6.9 Conclusions: Resolution Correction
- 6.10 References
- Appendix 1: Example of an LC Non-Linear Regression Application: Use of the Nelder-Mead Simplex Search to Fit a Gaussian Shape to an Experimental Chromatogram
- Appendix 2: Solvent Strength in the Snyder-Glajch-Kirkland Triangular Composition Diagram
- Nomenclature
- Subject Index
