
Modern Methods in Solid-state NMR
A Practitioner's Guide
Paul Hodgkinson(Editor)
Royal Society of Chemistry (Publisher)
Published on 9. April 2018
Book
Hardback
456 pages
978-1-78262-854-5 (ISBN)
Description
Solid-state NMR covers an enormous range of material types and experimental techniques. Although the basic instrumentation and techniques of solids NMR are readily accessible, there can be significant barriers, even for existing experts, to exploring the bewildering array of more sophisticated techniques. In this unique volume, a range of experts in different areas of modern solid-state NMR explain about their area of expertise, emphasising the "practical aspects" of implementing different techniques, and illustrating what questions can and cannot be addressed. Later chapters address complex materials, showing how different NMR techniques discussed in earlier chapters can be brought together to characterise important materials types. The volume as a whole focusses on topics relevant to the developing field of "NMR crystallography" - the use of solids NMR as a complement to diffraction crystallography.
This book is an ideal complement to existing introductory texts and reviews on solid-state NMR. New researchers wanting to understand new areas of solid-state NMR will find each chapter to be the equivalent to spending time in the laboratory of an internationally leading expert, learning the hints and tips that make the difference between knowing about a technique and being ready to put it into action. With no equivalent on the market, it will be of interest to every solid-state NMR researcher (academic and postgraduate) working in the chemical sciences.
This book is an ideal complement to existing introductory texts and reviews on solid-state NMR. New researchers wanting to understand new areas of solid-state NMR will find each chapter to be the equivalent to spending time in the laboratory of an internationally leading expert, learning the hints and tips that make the difference between knowing about a technique and being ready to put it into action. With no equivalent on the market, it will be of interest to every solid-state NMR researcher (academic and postgraduate) working in the chemical sciences.
More details
Series
Language
English
Place of publication
Cambridge
United Kingdom
Target group
Professional and scholarly
Product notice
Unsewn / adhesive bound
Dimensions
Height: 234 mm
Width: 156 mm
Thickness: 23 mm
Weight
829 gr
ISBN-13
978-1-78262-854-5 (9781782628545)
Copyright in bibliographic data and cover images is held by Nielsen Book Services Limited or by the publishers or by their respective licensors: all rights reserved.
Schweitzer Classification
Other editions
Additional editions

E-Book
04/2018
1st Edition
Royal Society of Chemistry
€231.99
Available for download

E-Book
04/2018
1st Edition
Royal Society of Chemistry
€233.99
Available for download
Person
Dr Paul Hodgkinson is a Reader in Magnetic Resonance at Durham University, UK. His research combines interests in technique development and methodology in solid-state NMR as well as applications to chemical problems. Applications of NMR have been in the area of structural chemistry, particularly of pharmaceutical materials and systems with mobility, such as soft solids and solvates. A particular interest is in combining information from diffraction-based experiments, NMR and computation of NMR parameters (using DFT codes), and dynamics (molecular dynamics simulations).
Content
Heteronuclear Correlation SSNMR Spectroscopy with Indirect Detection under Fast Magic-Angle Spinning;
High-resolution 1H 2D MAS techniques for organic solids;
Isotropic vs. anisotropic chemical shift separation;
Two-dimensional methods for half-integer quadrupolar nuclei;
14N Solid-State NMR;
CODEX-based Methods for Studying Slow Dynamics;
NMR Studies of Ionic Dynamics in Solids;
Low-Temperature NMR: Techniques and Applications;
NMR at High Temperature;
Isotopically Enriched Systems;
NMR Studies of Electrochemical Storage Materials;
Disordered Solids;
Characterization of Liquid-Crystalline Materials by Separated Local Field Methods
High-resolution 1H 2D MAS techniques for organic solids;
Isotropic vs. anisotropic chemical shift separation;
Two-dimensional methods for half-integer quadrupolar nuclei;
14N Solid-State NMR;
CODEX-based Methods for Studying Slow Dynamics;
NMR Studies of Ionic Dynamics in Solids;
Low-Temperature NMR: Techniques and Applications;
NMR at High Temperature;
Isotopically Enriched Systems;
NMR Studies of Electrochemical Storage Materials;
Disordered Solids;
Characterization of Liquid-Crystalline Materials by Separated Local Field Methods