Organic Syntheses, Volume 77
1st Edition
Published on 22. September 2000
Book
Hardback
352 pages
978-0-471-39567-6 (ISBN)
Description
Organic Syntheses, Volume 77 describes twenty-eight checked and edited experimental procedures, spanning a broad range of synthetic methodologies, and provides chemists with a compendium of new or little known experimental procedures which lead to useful compounds or that illustrate important new developments in methodology. For every procedure, safety warnings are presented along with detailed descriptions for the preparation, purification, and identification of the compound in question. Additionally, special reaction conditions are detailed, along with the source of reagents, helpful waste disposal guidelines, discussions of results, references to the primary literature, and an appendix of nomenclature and registry numbers. Coverage is divided into four main sections devoted to: reagents and procedures for asymmetric synthesis; chemical processes; chemical reagents; and chemical compounds, respectively.
More details
Series
Language
English
Place of publication
New York
United States
Target group
College/higher education
Professional and scholarly
Dimensions
Height: 233 mm
Width: 160 mm
Thickness: 21 mm
Weight
640 gr
ISBN-13
978-0-471-39567-6 (9780471395676)
Copyright in bibliographic data and cover images is held by Nielsen Book Services Limited or by the publishers or by their respective licensors: all rights reserved.
Schweitzer Classification
Person
David J. Hart is the author of Organic Syntheses, Volume 77, published by Wiley.
Content
Partial table of contents:Preparation of (R,R)-1,2:4,5-Diepoxypentane (S. Rychnovsky, et al.).
Synthesis and Diastereoselective Alkylation of Pseudoephedrine Amides (A. Myers & B. Yang).
(R)-(+)-2-Hydroxy-1,2,2-Triphenylethyl Acetate (J. Macor, et al.).
Synthesis of 1,1-Dimethylethyl (S)-4-Formyl-2,2-Dimethyl-3-Oxazolidinecarboxylate By Reduction of the Alcohol (A. Dondoni & D. Perrone).
Synthesis of (S,E)-1-(Methoxymethoxy)-1-Tributylstannyl-2-Butene (J. Marshall, et al.).
Allylindation in Aqueous Media: Methyl 3-(Hydroxymethyl)-4-Methyl-2-Methylenepentanoate (G. Bennett & L. Paquette).
The Synthesis of 2-Alkyl-4-Pyrones From Meldrum's Acid (M. Crimmins, et al.).
9-Ethyl-3,6-Dimethylcarbazole (DMECZ) (J. Buck, et al.).
Bis(Pinacolato)Diboron (T. Ishiyama, et al.).
-Tosylbenzyl Isocyanide (J. Sisko, et al.).
Methyl 2,3-O-(6,6'-Octahydro-6,6'-Bi-2H-Pyran-2,2'-Diyl)--D-Galactopyranoside (S. Ley & H. Osborn).
Cyclopropylacetylene (E. Corley, et al.).
3-Nitropropanal, 3-Nitropropanol, and 3-Nitropropanal Dimethyl Acetal (H. Griesser, et al.).
Cyclopropene: A New Synthesis and Its Diels-Alder Reaction with Cyclopentadiene (P. Binger, et al.).
Unchecked Procedures.
Indexes.
Synthesis and Diastereoselective Alkylation of Pseudoephedrine Amides (A. Myers & B. Yang).
(R)-(+)-2-Hydroxy-1,2,2-Triphenylethyl Acetate (J. Macor, et al.).
Synthesis of 1,1-Dimethylethyl (S)-4-Formyl-2,2-Dimethyl-3-Oxazolidinecarboxylate By Reduction of the Alcohol (A. Dondoni & D. Perrone).
Synthesis of (S,E)-1-(Methoxymethoxy)-1-Tributylstannyl-2-Butene (J. Marshall, et al.).
Allylindation in Aqueous Media: Methyl 3-(Hydroxymethyl)-4-Methyl-2-Methylenepentanoate (G. Bennett & L. Paquette).
The Synthesis of 2-Alkyl-4-Pyrones From Meldrum's Acid (M. Crimmins, et al.).
9-Ethyl-3,6-Dimethylcarbazole (DMECZ) (J. Buck, et al.).
Bis(Pinacolato)Diboron (T. Ishiyama, et al.).
-Tosylbenzyl Isocyanide (J. Sisko, et al.).
Methyl 2,3-O-(6,6'-Octahydro-6,6'-Bi-2H-Pyran-2,2'-Diyl)--D-Galactopyranoside (S. Ley & H. Osborn).
Cyclopropylacetylene (E. Corley, et al.).
3-Nitropropanal, 3-Nitropropanol, and 3-Nitropropanal Dimethyl Acetal (H. Griesser, et al.).
Cyclopropene: A New Synthesis and Its Diels-Alder Reaction with Cyclopentadiene (P. Binger, et al.).
Unchecked Procedures.
Indexes.