Split and Splitless Injection for Quantitative Gas Chromatography
Concepts, Processes, Practical Guidelines, Sources of Error
4th Edition
Published on 7. March 2001
Book
Hardback
480 pages
978-3-527-29879-2 (ISBN)
Description
This comprehensive and unique handbook of split and splitless injection techniques has been completely revised and updated.
- New insights concerning sample evaporation in the injector
- Consequences of matrix effects
- A new chapter on injector design
The real processes within the injector are for the first time visualized and explained by the CD-ROM included in the book.
Reviews / Votes
From reviews of former editions: "This substantial book is on injection techniques alone, which...demonstrates can have many pitfalls...no one should be allowed to direct a laboratory doing quantitative analysis by GC without first being thoroughly familar with this book..." (The Analyst) "This is a detailed reference volume filled with practical suggestions and techniques for managing split and splitless injection in the day--to--day world of the working gas chromatographer. It will be useful...for anyone who must work hands--on with GC." (Journal of High Resolution Chromatography) Reviews of 4th editions: "...examines the critical details of injector design and the often significant differences in their essential parts." (SciTech Book News, Vol. 26, No. 2, June 2002) "...This volume provides a valuable insight into the operating principles and mechanics of GC systems"... (Carbohydrate Polymers, Vol.53, 2003)More details
Edition
4., vollst. überarb. Aufl.
Language
English
Place of publication
Weinheim
Germany
Target group
College/higher education
Professional and scholarly
Laboratorien, analytische, Laboratorien, chemische, Laboratorien, pharmazeutische, Analytiker, Chromatographen
Edition type
Revised edition
Illustrations
175 s/w Abbildungen, 33 s/w Tabellen
Illustrations
Dimensions
Height: 24 cm
Width: 17 cm
Weight
1081 gr
ISBN-13
978-3-527-29879-2 (9783527298792)
Schweitzer Classification
Other editions
Additional editions
Konrad Grob
Split and Splitless Injection for Quantitative Gas Chromatography
Concepts, Processes, Practical Guidelines, Sources of Error
E-Book
11/2008
4th Edition
Wiley-VCH
€165.99
Available for download
Previous edition
Konrad Grob
Split and Splitless Injection in Capillary Gas Chromatography
With Some Remarks on PTV Injection
Book
06/1993
3rd Edition
Wiley-VCH
€61.90
Article exhausted; check for reprint
Person
K. Grob, Kantonales Labor Zürich, Switzerland
Content
PART A: SYRINGE NEEDLE. Syringe Needle Handling Techniques. Evaporation Inside Needle. Possibilities of Avoiding Evaporation in the Needle. Sample Volume. Solvents and Solutes. PART B: SAMPLE EVAPORATION IN THE INJECTOR. Vaporizing Chamber. Evaporation Time. Amount of Heat Required. Sources of Heat. Problems Caused by Incomplete Evaporation. PART C: SPLIT INJECTION. The Split Ratio. Sample Concentration Suitable for Split Injection. Split Injection for Fast Analysis. Analysis Requiring Maximum Sensitivity. High Split Ratios for Reducing Sample Size. Problems Concerning the Split Ratio. Problems Concerning the Linearity of Splitting. PART D: SPLITLESS INJECTION. How to Perform Splitless Injection. Sample Volumes Suitable for Splitless Injection. Splitless Injection of Large Volumes. General Evaluation of Splitless Injection. PART E: INJECTOR DESIGN. Design for Split Injection Design for Splitless Injection.