Spin-1 NMR
Published on 27. September 2011
Book
Paperback/Softback
VIII, 122 pages
978-3-642-64689-8 (ISBN)
Description
The Basic Physics of Spin-1 Systems.- 1.1 General Introduction.- 1.2 Spin States and Matrix Representations of Operators for Spin-1.- 1.3 Spin-1 Operator Algebra.- 1.4 L¿wdin Projectors for Spin-1.- 1.5 Interactions Relevant in Spin-1 NMR.- 1.6 Pulse Rotations.- 1.7 Density Matrix Description of the State of Spin-1 Ensembles.- 1.8 Evolution of the Spin-1 System Under Quadrupolar Coupling.- 1.9 Phase Changes of Spin-1 Wavefunctions Under Rotation.- 1.10 Evolution of the Spin-1-Spin-1/2 System Under Scalar Coupling.- 1.11 Spin Tickling in a Spin-l/2-Spin-l Scalar Coupled System.- 1.12 Evolution of the Spin-l-Spin-1 System Under Scalar Coupling.- 1.13 Coherence Transfer Function for Spin-1 Systems.- 1.14 Quadrupolar Relaxation.- 1.15 Spin-1 Behavior of Two Equivalent Spins-1/2.- NMR of Systems Involving Spin-1 Nuclei in the Isotropic Phase..- 2.1 Chemical Shift Information.- 2.2 General Spectral Features Consequent on Coupling to Spin-1.- 2.3 Laboratory Frame Polarization Transfer Involving Spin-1 Nuclei.- 2.4 INEPT Polarization Transfer from Spin-1 (S) to Spin-1/2 (I).- 2.5 DEPT Polarization Transfer from Spin-1 (S) to Spin-1/2 (I).- 2.6 Polarization Transfer from Spin-1/2 (I) to Spin-1 (S).- 2.7 Pulse Width Calibration for Polarization Transfer Experiments.- 2.8 Polarization Transfer Between Spin-1 Nuclei.- 2.9 Two-Dimensional Experiments Involving Spin-1 Nuclei.- 2.10 Correlation Spectroscopy (COSY).- 2.11 Heteronuclear Multiple Quantum Spectroscopy.- 2.12 Homonuclear Multiple Quantum Spectroscopy.- 2.13 Relayed Correlation Spectroscopy.- 2.14 Instrumentation for High Resolution Spin-1 NMR.- 3 NMR of Spin-1 Systems in the Solid State.- 3.1 Introduction.- 3.2 Quadrupolar Echo.- 3.3 Jeener-Broekaert Sequence.- 3.4 Deuterium NMR Spectroscopy of Single Crystal Systems.- 3.5 Two-Dimensional Deuterium COSY Spectra in the Solid State.- 3.6 Deuterium NMR Under Magic Angle Spinning.- 3.7 Double Quantum Spectroscopy.- 3.8 QUADSHIFT Experiment.- 3.9 Overtone Spectroscopy.- 3.10 Spin-1/2-Spin-1 Dipolar Coupling.- 3.11 Spin Alignment.- 3.12 Deuterium Exchange Spectroscopy in Single Crystals.- 3.13 Deuterium Exchange Spectroscopy.- 3.14 Spin-1 Double Quantum Imaging.- 3.15 Instrumentation for Solid State NMR.- 4 Reference.
Reviews / Votes
"For someone just entering the field this work provides a clear introduction covering all aspects...For experts it provides an up-to-date course of references." Applied MAGNETIC ResonanceMore details
Series
Edition
Softcover reprint of the original 1st ed. 1996
Language
English
Place of publication
Berlin
Germany
Publishing group
Springer Berlin
Target group
Professional and scholarly
Research
Illustrations
VIII, 122 p.
Dimensions
Height: 235 mm
Width: 155 mm
Thickness: 8 mm
Weight
219 gr
ISBN-13
978-3-642-64689-8 (9783642646898)
DOI
10.1007/978-3-642-61089-9
Schweitzer Classification
Other editions
Additional editions
Persons
Content
The Basic Physics of Spin-1 Systems.- 1.1 General Introduction.- 1.2 Spin States and Matrix Representations of Operators for Spin-1.- 1.3 Spin-1 Operator Algebra.- 1.4 Löwdin Projectors for Spin-1.- 1.5 Interactions Relevant in Spin-1 NMR.- 1.6 Pulse Rotations.- 1.7 Density Matrix Description of the State of Spin-1 Ensembles.- 1.8 Evolution of the Spin-1 System Under Quadrupolar Coupling.- 1.9 Phase Changes of Spin-1 Wavefunctions Under Rotation.- 1.10 Evolution of the Spin-1-Spin-1/2 System Under Scalar Coupling.- 1.11 Spin Tickling in a Spin-l/2-Spin-l Scalar Coupled System.- 1.12 Evolution of the Spin-l-Spin-1 System Under Scalar Coupling.- 1.13 Coherence Transfer Function for Spin-1 Systems.- 1.14 Quadrupolar Relaxation.- 1.15 Spin-1 Behavior of Two Equivalent Spins-1/2.- NMR of Systems Involving Spin-1 Nuclei in the Isotropic Phase..- 2.1 Chemical Shift Information.- 2.2 General Spectral Features Consequent on Coupling to Spin-1.- 2.3 Laboratory Frame Polarization Transfer Involving Spin-1 Nuclei.- 2.4 INEPT Polarization Transfer from Spin-1 (S) to Spin-1/2 (I).- 2.5 DEPT Polarization Transfer from Spin-1 (S) to Spin-1/2 (I).- 2.6 Polarization Transfer from Spin-1/2 (I) to Spin-1 (S).- 2.7 Pulse Width Calibration for Polarization Transfer Experiments.- 2.8 Polarization Transfer Between Spin-1 Nuclei.- 2.9 Two-Dimensional Experiments Involving Spin-1 Nuclei.- 2.10 Correlation Spectroscopy (COSY).- 2.11 Heteronuclear Multiple Quantum Spectroscopy.- 2.12 Homonuclear Multiple Quantum Spectroscopy.- 2.13 Relayed Correlation Spectroscopy.- 2.14 Instrumentation for High Resolution Spin-1 NMR.- 3 NMR of Spin-1 Systems in the Solid State.- 3.1 Introduction.- 3.2 Quadrupolar Echo.- 3.3 Jeener-Broekaert Sequence.- 3.4 Deuterium NMR Spectroscopy of Single Crystal Systems.-3.5 Two-Dimensional Deuterium COSY Spectra in the Solid State.- 3.6 Deuterium NMR Under Magic Angle Spinning.- 3.7 Double Quantum Spectroscopy.- 3.8 QUADSHIFT Experiment.- 3.9 Overtone Spectroscopy.- 3.10 Spin-1/2-Spin-1 Dipolar Coupling.- 3.11 Spin Alignment.- 3.12 Deuterium Exchange Spectroscopy in Single Crystals.- 3.13 Deuterium Exchange Spectroscopy.- 3.14 Spin-1 Double Quantum Imaging.- 3.15 Instrumentation for Solid State NMR.- 4 Reference.