Organic Structures from Spectra

 
 
Wiley (Verlag)
  • 4. Auflage
  • |
  • erschienen am 7. September 2011
  • |
  • 468 Seiten
 
E-Book | ePUB mit Adobe DRM | Systemvoraussetzungen
978-1-119-96461-2 (ISBN)
 
Organic Structures from Spectra, Fourth Edition consists ofa carefully selected set of over 300 structural problems involvingthe use of all the major spectroscopic techniques. The problems aregraded to develop and consolidate the student's understandingof Organic Spectroscopy, with the accompanying text outliningthe basic theoretical aspects of major spectroscopictechniques at a level sufficient to tackle the problems.
Specific changes for the new edition will include
* A significantly expanded section on 2D NMR spectroscopyfocusing on COSY, NOESY and CH-Correlation
* Incorporating new material into some tables to provide extracharacteristic data for various classes of compounds
* Additional basic information on how to solve spectroscopicproblems
* Providing new problems within the area of 10 2D NMRspectroscopy
* More problems at the 'simpler' end of therange
As with previous editions, this book combines basic theory,practical advice and sensible approaches to solving spectraproblems. It will therefore continue to prove invaluable tostudents studying organic spectroscopy across a range ofdisciplines.
4. Auflage
  • Englisch
John Wiley & Sons
  • 22,94 MB
978-1-119-96461-2 (9781119964612)
111996461X (111996461X)
weitere Ausgaben werden ermittelt
PREFACE.
LIST OF TABLES.
LIST OF FIGURES.
1 INTRODUCTION.
1.1 GENERAL PRINCIPLES OF ABSORPTION SPECTROSCOPY.
1.2 CHROMOPHORES.
1.3 DEGREE OF UNSATURATION.
1.4 CONNECTIVITY.
1.5 SENSITIVITY.
1.6 PRACTICAL CONSIDERATIONS.
2 ULTRAVIOLET (UV) SPECTROSCOPY.
2.1 BASIC INSTRUMENTATION.
2.2 THE NATURE OF ULTRAVIOLET SPECTROSCOPY.
2.3 QUANTITATIVE ASPECTS OF ULTRAVIOLET SPECTROSCOPY.
2.4 CLASSIFICATION OF UV ABSORPTION BANDS.
2.5 SPECIAL TERMS IN ULTRAVIOLET SPECTROSCOPY.
2.6 IMPORTANT UV CHROMOPHORES.
2.7 THE EFFECT OF SOLVENTS.
3 INFRARED (IR) SPECTROSCOPY.
3.1 ABSORPTION RANGE AND THE NATURE OF IR ABSORPTION.
3.2 EXPERIMENTAL ASPECTS OF INFRARED SPECTROSCOPY.
3.3 GENERAL FEATURES OF INFRARED SPECTRA.
3.4 IMPORTANT IR CHROMOPHORES.
4 MASS SPECTROMETRY.
4.1 IONIZATION PROCESSES.
4.2 INSTRUMENTATION.
4.3 MASS SPECTRAL DATA.
4.4 REPRESENTATION OF FRAGMENTATION PROCESSES.
4.5 FACTORS GOVERNING FRAGMENTATION PROCESSES.
4.6 EXAMPLES OF COMMON TYPES OF FRAGMENTATION.
5 NUCLEAR MAGNETIC RESONANCE (NMR) SPECTROSCOPY.
5.1 THE PHYSICS OF NUCLEAR SPINS AND NMR INSTRUMENTS.
5.2 CONTINUOUS WAVE (CW) NMR SPECTROSCOPY.
5.3 FOURIER-TRANSFORM (FT) NMR SPECTROSCOPY.
5.4 CHEMICAL SHIFT IN 1H NMR SPECTROSCOPY.
5.5 SPIN-SPIN COUPLING IN 1H NMR SPECTROSCOPY.
5.6 ANALYSIS OF 1H NMR SPECTRA.
5.7 RULES FOR SPECTRAL ANALYSIS.
6 13C NMR SPECTROSCOPY.
6.1 COUPLING AND DECOUPLING IN 13C NMR SPECTRA.
6.2 DETERMINING 13C SIGNAL MULTIPLICITY USING DEPT.
6.3 SHIELDING AND CHARACTERISTIC CHEMICAL SHIFTS IN 13C NMRSPECTRA.
7 MISCELLANEOUS TOPICS.
7.1 DYNAMIC PROCESSES IN NMR - THE NMR TIME-SCALE.
7.2 THE EFFECT OF CHIRALITY.
7.3 THE NUCLEAR OVERHAUSER EFFECT (NOE).
7.4 TWO DIMENSIONAL NMR.
7.5 THE NMR SPECTRA OF "OTHER NUCLEI".
7.6 SOLVENT - INDUCED SHIFTS.
8 DETERMINING THE STRUCTURE OF ORGANIC MOLECULES FROMSPECTRA.
9 PROBLEMS.
9.1 ORGANIC STRUCTURES FROM SPECTRA.
9.2 THE ANALYSIS OF MIXTURES.
9.3 PROBLEMS IN 2-DIMENSIONAL NMR.
9.4 NMR SPECTRAL ANALYSIS.
APPENDIX.
INDEX.

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